WebApr 12, 2024 · The uptake of gaseous iodine into the crystalline sponge material [(ZnI2)3(tpt)2]·0.7triphenylene·0.3PhNO2·0.7C6H12 1 (tpt = 2,4,6-tris(4-pyridyl)-1,3,5-triazine) has been monitored by dynamic X-ray diffraction and thermogravimetric analysis. The X-ray analyses have enabled the location, quantity, uptake rate, and subsequent … WebNov 22, 2024 · Crystalline Sponge Method: X-ray Structure Analysis of Small Molecules by Post-Orientation within Porous Crystals-Principle and Proof-of-Concept Studies Angew Chem Int Ed Engl. 2024 Nov 22;60 (48):25204-25222. doi: 10.1002/anie.202406265. Epub 2024 Aug 3. Authors Nicolas Zigon 1 , Vincent Duplan 1 , Naoki Wada 1 , Makoto Fujita …
The Crystalline Sponge Method: Enhancing the Technique for …
WebThe Crystalline Sponge (CS) method is an approach to obtain single-crystal X-ray structures of compounds, that are difficult or impossible to crystallize, for example because they are of too small a quantity, are not solid at ambient conditions or … WebFeb 7, 2024 · The crystalline sponge method has shown to be a novel strategy for structure determination of non-crystalline, oily or trace amount of compound. The target … church work day logo
The updated crystalline sponge method - Phys.org
WebNov 11, 2024 · Crystalline sponges can help pharmaceutical companies, assess and manage metabolite-related risks, earlier and more efficiently and help them avoid costly problems later on, like having to stop a late stage … Web1 day ago · A new type of crystalline solid, termed "solvate sponge crystal" is presented, and the chemical basis of its properties are explained for a melt-and press-castable solid sodium-ion conductor. WebApr 1, 2024 · The crystalline sponge method allowed for complete structure elucidation of the known metabolites S - trans -4'-hydroxy-PZQ (M1), S - cis -4'-hydroxy-PZQ (M2) and S -/ R -11b-hydroxy-PZQ (M6) as well as the unknown metabolites S -9-hydroxy-PZQ (M3) and S -7-hydroxy- S -PZQ (M4). dfe webinar single central record